[Objective] The paper was to establish the method for quantitative analysis of glyphosate herbicide and identification of salt type. [Method] Using ion chromatographic column switching method,cations( sodion,ammonium ...[Objective] The paper was to establish the method for quantitative analysis of glyphosate herbicide and identification of salt type. [Method] Using ion chromatographic column switching method,cations( sodion,ammonium ion,potassium ion,dimethonium ion and isopropylamine ion) and glyphosate anion in glyphosate salt were determined with Thermo IonP ac SCS1 cation exchange column and Thermo IonP ac AS14 anion exchange column,and external standard method was used for quantification. [Result] Various components showed good linear relationship within the linearity range,and the correlation coefficient r was greater than 0. 999; the relative standard deviation of retention time and peak area were less than 0. 13% and 1. 22%,respectively; the recovery was 98. 22%-99. 97%.[Conclusion] The method is precise,accurate and simple,and can be used to determine the active ingredients of glyphosate herbicide.展开更多
In order to compensate the dispersion accumulated in a single mode fiber(SMF)for higher communication capacity,a simplified dispersion-compensation microstructure fiber(DC-MSF)with seven cores is proposed in this pape...In order to compensate the dispersion accumulated in a single mode fiber(SMF)for higher communication capacity,a simplified dispersion-compensation microstructure fiber(DC-MSF)with seven cores is proposed in this paper.The fiber’s cladding is made of pure silica without air holes,and its outer cores are composed of six germanium up-doped cylinders,which has the advantage of simple structure.The finite element method(FEM)and beam propagation method(BPM)are used to study the properties of the fiber,and the relationship between the structural parameters of the fiber and the dispersion,as well as the phase matching wavelength,is obtained.By optimizing the structural parameters of the fiber,the dispersion of the fiber can reach-5291.47 ps·nm^(-1)·km^(-1) at 1550 nm,and the coupling loss to the conventional single-mode fiber is only 0.137 d B.Compared with the conventional dispersion-compensation fiber,the fiber has lots of advantages,such as single mode transmission,easy to fabricate and low coupling loss with traditional SMF,etc.展开更多
基金Supported by Science and Technology Project of Zhejiang Province(2016C37034)
文摘[Objective] The paper was to establish the method for quantitative analysis of glyphosate herbicide and identification of salt type. [Method] Using ion chromatographic column switching method,cations( sodion,ammonium ion,potassium ion,dimethonium ion and isopropylamine ion) and glyphosate anion in glyphosate salt were determined with Thermo IonP ac SCS1 cation exchange column and Thermo IonP ac AS14 anion exchange column,and external standard method was used for quantification. [Result] Various components showed good linear relationship within the linearity range,and the correlation coefficient r was greater than 0. 999; the relative standard deviation of retention time and peak area were less than 0. 13% and 1. 22%,respectively; the recovery was 98. 22%-99. 97%.[Conclusion] The method is precise,accurate and simple,and can be used to determine the active ingredients of glyphosate herbicide.
基金supported by the Natural Science Foundation of Hebei Province(No.F2021203002)the Science and Technology Project of Hebei Education Department(No.ZD2021409)+2 种基金the Research Projects of Talent Project Training Funds of Hebei Province(No.C20221067)the Talent Project of Tangshan City(No.A202110009)the Science and Technology Project of Tangshan City(No.22130216G)。
文摘In order to compensate the dispersion accumulated in a single mode fiber(SMF)for higher communication capacity,a simplified dispersion-compensation microstructure fiber(DC-MSF)with seven cores is proposed in this paper.The fiber’s cladding is made of pure silica without air holes,and its outer cores are composed of six germanium up-doped cylinders,which has the advantage of simple structure.The finite element method(FEM)and beam propagation method(BPM)are used to study the properties of the fiber,and the relationship between the structural parameters of the fiber and the dispersion,as well as the phase matching wavelength,is obtained.By optimizing the structural parameters of the fiber,the dispersion of the fiber can reach-5291.47 ps·nm^(-1)·km^(-1) at 1550 nm,and the coupling loss to the conventional single-mode fiber is only 0.137 d B.Compared with the conventional dispersion-compensation fiber,the fiber has lots of advantages,such as single mode transmission,easy to fabricate and low coupling loss with traditional SMF,etc.
