The present work investigates the microstructural evolution and mechanical properties in a novel medium-Si 12%Cr reduced activation ferritic/martensitic steel cladding tube(Fe-11.8Cr-0.2C-1.4W-0.17Ta-0.2V-0.55Si-0.5Mn...The present work investigates the microstructural evolution and mechanical properties in a novel medium-Si 12%Cr reduced activation ferritic/martensitic steel cladding tube(Fe-11.8Cr-0.2C-1.4W-0.17Ta-0.2V-0.55Si-0.5Mn,wt%)during multipass cold rolling and annealing.The initial hot-extruded tube exhibited a full martensitic matrix with the prior austenite grain size of~32μm.After annealing,Cr_(23)C_(6) and TaC particles were precipitated,which are basically unchanged(152-183 nm and 84-113 nm,respectively)during the manufacturing process.Meanwhile,with the cold-rolling strain(ε)increasing and subsequent annealing,the martensitic lath gradually diminishes,and the recrystallization volume fraction(f_(r))is increased.Based on the static recrystallization kinetics model,a clear relationship between f_(r) andεis established,in which the newly proposed kinetic equation demonstrates a strong correlation with the experimental results.Furthermore,the yield strength(σ_(YS)=362 MPa)of the final annealed state was much lower than that(σ_(YS)=482 MPa)of the initial annealed state,which can be attributed to the recrystallization from the martensitic matrix to ferritic matrix.Various strengthening mechanisms are further discussed,and the calculated strengths are in good agreement with the experimental results.This work provides a guidance for the optimization of cold-rolling and annealing treatments in the manufacture of cladding tube.展开更多
基金supported by the National Natural Science Foundation of China(No.52171152).
文摘The present work investigates the microstructural evolution and mechanical properties in a novel medium-Si 12%Cr reduced activation ferritic/martensitic steel cladding tube(Fe-11.8Cr-0.2C-1.4W-0.17Ta-0.2V-0.55Si-0.5Mn,wt%)during multipass cold rolling and annealing.The initial hot-extruded tube exhibited a full martensitic matrix with the prior austenite grain size of~32μm.After annealing,Cr_(23)C_(6) and TaC particles were precipitated,which are basically unchanged(152-183 nm and 84-113 nm,respectively)during the manufacturing process.Meanwhile,with the cold-rolling strain(ε)increasing and subsequent annealing,the martensitic lath gradually diminishes,and the recrystallization volume fraction(f_(r))is increased.Based on the static recrystallization kinetics model,a clear relationship between f_(r) andεis established,in which the newly proposed kinetic equation demonstrates a strong correlation with the experimental results.Furthermore,the yield strength(σ_(YS)=362 MPa)of the final annealed state was much lower than that(σ_(YS)=482 MPa)of the initial annealed state,which can be attributed to the recrystallization from the martensitic matrix to ferritic matrix.Various strengthening mechanisms are further discussed,and the calculated strengths are in good agreement with the experimental results.This work provides a guidance for the optimization of cold-rolling and annealing treatments in the manufacture of cladding tube.