The fact is that Nigeria ceramic raw materials are underutilized as a result of inadequate information on the materials which limits the local production of water closet. The emphasis of this research was on the suita...The fact is that Nigeria ceramic raw materials are underutilized as a result of inadequate information on the materials which limits the local production of water closet. The emphasis of this research was on the suitability of the physio-chemical properties of the abundant locally sourced ceramic raw materials from South-west Nigeria. The selected locally sourced raw materials included: kaolin, feldspar, silica and ball clay. The Physical properties carried out on the specimens produced include chemical analysis, shrinkage, porosity, bulk density, modulus of rupture, plasticity and viscosity. The physical property tests were done in accordance with (ASTM C). Standard and the chemical composition were identified by AAS spectrometer. However, the ratio of kaolin, feldspar, quartz and ball clay was varied in five major formulation represented as A, B, C, D and E. The clay, kaolin, quartz and feldspar used in this study were found to belong to alumina-silicate group suitable for the production of standard water closet. The samples’ properties met the required standards;hence, the materials were found suitable for production of water closet of acceptable standards. Composition A specimen gives the most suitable proportions for the production of water closet at 40% of kaolin, 25% of feldspar, 10% of quartz and 25% of ball clay respectively.展开更多
A 13% chromium white iron was produced using a stir cast process. Samples of the produced white iron were austenised at 1450°C and then quenched in water to the room temperature. The characterisation tools such a...A 13% chromium white iron was produced using a stir cast process. Samples of the produced white iron were austenised at 1450°C and then quenched in water to the room temperature. The characterisation tools such as X-ray diffractometer, scanning electron microscope, Brinell hardness tester and pin on disc machine were employed in the studies of the phase orientation and morphology, hardness value measurement and investigation of wear behaviour. The results revealed that water quenching the 13% chromium white iron led to the precipitation of fine iron chromides and cementite in the matrix of martensite. Moreover, there is an about 22% to 45% increase in hardness values of the as-cast 13% chromium white iron as the %composition of graphite additions increased from 1.36 to 3.04. However, the impact energy values are sacrificed. The increase in hardness values is attributable to hard intermetallic compounds such as iron chromides and cementite phases in the iron matrix. Also, there is an about 32% - 42% increase in hardness values of the heat treated samples of 13% chromium white iron when compared with those of the as-cast. The increased hardness values are attributable to even distribution of the fine intermetallic compounds in the fine grains of martensitic matrix. The wear rate increased as the sliding moments per unit time increased due to increasing work done by the friction to oppose the rotation of the pin on disc. The water quenched 13% chromium white iron samples have greater wear resistances than the as-cast samples due to their greater hardness values than those of the as-cast samples. The effect of speed increase on decreasing wear resistances is more pronounced on the heat treated samples than on the as-cast samples. Hence, the water quenched 13% chromium white iron is an excellent material in application requiring high wear resistance and low impact energy especially in grinding mill liner plate, bottom or casing used in the concrete pipe production, roller for crushing and pulverising mills.展开更多
An alloy of cast iron and copper (Fe-Cu) has been developed using a stir cast process. The compo-sitional, microstructural characterization and wear property of the developed Fe-Cu alloy were carried out with the aids...An alloy of cast iron and copper (Fe-Cu) has been developed using a stir cast process. The compo-sitional, microstructural characterization and wear property of the developed Fe-Cu alloy were carried out with the aids of X-ray diffractometer, scanning electron microscope (SEM) and pin on Disc machine. The mechanical properties such as hardness and impact energy were investigated. Wear linear equations were generated with the aids of MATLAB linear fitting. The results revealed that the presence of copper (99% pure) in the melt of grey cast iron inhibited the formation of cementite. However, the impact energy of the grey cast iron increased with %weight (wt) of copper addition. Hence, the hardness and wear resistance of the developed Fe-Cu alloy were sacrificed. Hence, the developed Fe-Cu alloy is an excellent material which can be used in the vibration damping application especially in the shock absorber.展开更多
文摘The fact is that Nigeria ceramic raw materials are underutilized as a result of inadequate information on the materials which limits the local production of water closet. The emphasis of this research was on the suitability of the physio-chemical properties of the abundant locally sourced ceramic raw materials from South-west Nigeria. The selected locally sourced raw materials included: kaolin, feldspar, silica and ball clay. The Physical properties carried out on the specimens produced include chemical analysis, shrinkage, porosity, bulk density, modulus of rupture, plasticity and viscosity. The physical property tests were done in accordance with (ASTM C). Standard and the chemical composition were identified by AAS spectrometer. However, the ratio of kaolin, feldspar, quartz and ball clay was varied in five major formulation represented as A, B, C, D and E. The clay, kaolin, quartz and feldspar used in this study were found to belong to alumina-silicate group suitable for the production of standard water closet. The samples’ properties met the required standards;hence, the materials were found suitable for production of water closet of acceptable standards. Composition A specimen gives the most suitable proportions for the production of water closet at 40% of kaolin, 25% of feldspar, 10% of quartz and 25% of ball clay respectively.
文摘A 13% chromium white iron was produced using a stir cast process. Samples of the produced white iron were austenised at 1450°C and then quenched in water to the room temperature. The characterisation tools such as X-ray diffractometer, scanning electron microscope, Brinell hardness tester and pin on disc machine were employed in the studies of the phase orientation and morphology, hardness value measurement and investigation of wear behaviour. The results revealed that water quenching the 13% chromium white iron led to the precipitation of fine iron chromides and cementite in the matrix of martensite. Moreover, there is an about 22% to 45% increase in hardness values of the as-cast 13% chromium white iron as the %composition of graphite additions increased from 1.36 to 3.04. However, the impact energy values are sacrificed. The increase in hardness values is attributable to hard intermetallic compounds such as iron chromides and cementite phases in the iron matrix. Also, there is an about 32% - 42% increase in hardness values of the heat treated samples of 13% chromium white iron when compared with those of the as-cast. The increased hardness values are attributable to even distribution of the fine intermetallic compounds in the fine grains of martensitic matrix. The wear rate increased as the sliding moments per unit time increased due to increasing work done by the friction to oppose the rotation of the pin on disc. The water quenched 13% chromium white iron samples have greater wear resistances than the as-cast samples due to their greater hardness values than those of the as-cast samples. The effect of speed increase on decreasing wear resistances is more pronounced on the heat treated samples than on the as-cast samples. Hence, the water quenched 13% chromium white iron is an excellent material in application requiring high wear resistance and low impact energy especially in grinding mill liner plate, bottom or casing used in the concrete pipe production, roller for crushing and pulverising mills.
文摘An alloy of cast iron and copper (Fe-Cu) has been developed using a stir cast process. The compo-sitional, microstructural characterization and wear property of the developed Fe-Cu alloy were carried out with the aids of X-ray diffractometer, scanning electron microscope (SEM) and pin on Disc machine. The mechanical properties such as hardness and impact energy were investigated. Wear linear equations were generated with the aids of MATLAB linear fitting. The results revealed that the presence of copper (99% pure) in the melt of grey cast iron inhibited the formation of cementite. However, the impact energy of the grey cast iron increased with %weight (wt) of copper addition. Hence, the hardness and wear resistance of the developed Fe-Cu alloy were sacrificed. Hence, the developed Fe-Cu alloy is an excellent material which can be used in the vibration damping application especially in the shock absorber.
