The solvus temperature,volume fraction,coarsening behavior of γ＇ precipitates and the partitioning behavior of alloying elements as well as lattice misfit of γ/γ＇ phases influence the creep behavior of Ni-and Co-...The solvus temperature,volume fraction,coarsening behavior of γ＇ precipitates and the partitioning behavior of alloying elements as well as lattice misfit of γ/γ＇ phases influence the creep behavior of Ni-and Co-base superalloys.However,few investigations about the microstructural characteristics and the coarsening behavior of γ＇ precipitates were reported in multicomponent novel Co-base superalloys during thermal exposure.Two alloys containing different contents of molybdenum and tungsten have been investigated to explore the effect of molybdenum on γ＇ solvus temperature,γ ＋γ＇ microstructure and γ＇ coarsening in Co–Al–W–Ta–Ti-base alloys.The results showed that the γ＇ solvus temperature decreases with the addition of Mo.Mo addition reduces the Y＇ volume fractions after aging above 1000℃,but results in negligible influence on the γ＇ volume fractions aging at 900℃.Meanwhile,γ＇ coarsening is controlled by diffusion in experimental alloys after aging at 900℃ and 1000℃,and the kinetics of Y＇growth in experimental alloys are consistent with the predictions of LSW theory.展开更多
The effect of annealing treatment on the structure of CdS films was investigated. The cadmium sulfide thin films were prepared by chemical bath deposition, and were annealed at nitrogen atmosphere at different tempera...The effect of annealing treatment on the structure of CdS films was investigated. The cadmium sulfide thin films were prepared by chemical bath deposition, and were annealed at nitrogen atmosphere at different temperatures. The films were characterized by SEM and XPS (X-ray photoelectron spectroscopy). X-ray photoelectron spectroscopy was used to examine the chemical states on the CdS films surface. It was found that thermal annealing could produce large grains of CdS thin films, remove the air contamination and reduce the oxygen content on the CdS films surface. Therefore, the CdS films changed more uniform and smoother surface after thermal annealing.展开更多
基金financially supported by the National Natural Science Foundation of China (Grant Nos.50771012,51201006 and 51301014)the Aeronautical Science Foundation of China (Grant No.2009ZF74011)
文摘The solvus temperature,volume fraction,coarsening behavior of γ＇ precipitates and the partitioning behavior of alloying elements as well as lattice misfit of γ/γ＇ phases influence the creep behavior of Ni-and Co-base superalloys.However,few investigations about the microstructural characteristics and the coarsening behavior of γ＇ precipitates were reported in multicomponent novel Co-base superalloys during thermal exposure.Two alloys containing different contents of molybdenum and tungsten have been investigated to explore the effect of molybdenum on γ＇ solvus temperature,γ ＋γ＇ microstructure and γ＇ coarsening in Co–Al–W–Ta–Ti-base alloys.The results showed that the γ＇ solvus temperature decreases with the addition of Mo.Mo addition reduces the Y＇ volume fractions after aging above 1000℃,but results in negligible influence on the γ＇ volume fractions aging at 900℃.Meanwhile,γ＇ coarsening is controlled by diffusion in experimental alloys after aging at 900℃ and 1000℃,and the kinetics of Y＇growth in experimental alloys are consistent with the predictions of LSW theory.
基金The financial support was provided by the National High Technology Research and Development Program of China(Grant No.2001AA513011).
文摘The effect of annealing treatment on the structure of CdS films was investigated. The cadmium sulfide thin films were prepared by chemical bath deposition, and were annealed at nitrogen atmosphere at different temperatures. The films were characterized by SEM and XPS (X-ray photoelectron spectroscopy). X-ray photoelectron spectroscopy was used to examine the chemical states on the CdS films surface. It was found that thermal annealing could produce large grains of CdS thin films, remove the air contamination and reduce the oxygen content on the CdS films surface. Therefore, the CdS films changed more uniform and smoother surface after thermal annealing.
