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PCL/HA静电纺丝纤维涂层对可降解Mg/HA复合材料的表面改性:力学性能、腐蚀和生物相容性 被引量:1
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作者 M.SHAMSI m.sedighi A.BAGHERI 《Transactions of Nonferrous Metals Society of China》 SCIE EI CAS CSCD 2024年第5期1470-1486,共17页
采用搅拌铸造和挤压法制备Mg/HA复合材料,并在其表面采用静电纺丝法涂覆聚己内酯/羟基磷灰石(PCL/HA)纤维(2.5%和5%HA,质量分数),以提高其耐腐蚀性。力学性能测试结果表明,复合材料的压缩屈服强度从73MPa(纯镁)提高到151MPa,提高了107%... 采用搅拌铸造和挤压法制备Mg/HA复合材料,并在其表面采用静电纺丝法涂覆聚己内酯/羟基磷灰石(PCL/HA)纤维(2.5%和5%HA,质量分数),以提高其耐腐蚀性。力学性能测试结果表明,复合材料的压缩屈服强度从73MPa(纯镁)提高到151MPa,提高了107%。SEM、EDS和XRD分析表明,HA颗粒分布在多孔涂层中。极化曲线结果表明,涂层试样的耐腐蚀性能均优于未涂覆试样。PCL涂层使样品的腐蚀电流密度降低了两个数量级。通过极化和体外腐蚀试验证明了HA在涂层中的有效性。涂层和随后形成的Ca-P层阻碍了模拟体液与基体的接触和渗透,从而起到保护表面的作用。PCL/2.5%HA涂层样品的腐蚀速率最低,其平均值为0.98mm/a,与未涂层样品相比,在14天内减少了81%。根据3天MTT结果,使用PCL/2.5%HA涂层可使细胞活性从43%提高到121%。综上,涂覆PCL/2.5%HA纤维的Mg/HA复合材料在生物可吸收植入物方面具有广阔的应用前景。 展开更多
关键词 镁基复合材料 复合涂层 生物可降解 羟基磷灰石 聚己内酯纤维
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Severe plastic deformation (SPD) of biodegradable magnesium alloys and composites: A review of developments and prospects 被引量:19
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作者 M.Kasaeian-Naeini m.sedighi R.Hashemi 《Journal of Magnesium and Alloys》 SCIE EI CAS CSCD 2022年第4期938-955,共18页
The use of magnesium in orthopedic and cardiovascular applications has been widely attracted by diminishing the risk of abnormal interaction of the implant with the body tissue and eliminating the second surgery to re... The use of magnesium in orthopedic and cardiovascular applications has been widely attracted by diminishing the risk of abnormal interaction of the implant with the body tissue and eliminating the second surgery to remove it from the body.Nevertheless,the fast degradation rate and generally inhomogeneous corrosion subsequently caused a decline in the mechanical strength of Mg during the healing period.Numerous researches have been conducted on the influences of various severe plastic deformation(SPD)processes on magnesium bioalloys and biocomposites.This paper strives to summarize the various SPD techniques used to achieve magnesium with an ultrafine-grained(UFG)structure.Moreover,the effects of various severe plastic deformation methods on magnesium microstructure,mechanical properties,and corrosion behavior have been discussed.Overall,this review intends to clarify the different potentials of applying SPD processes to the magnesium alloys and composites to augment their usage in biomedical applications. 展开更多
关键词 MAGNESIUM Severe plastic deformation Biodegradable implant Mechanical properties Corrosion
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Effect of nano-sized Al2O3 reinforcing particles on uniaxial and high cycle fatigue behaviors of hot-forged AZ31B magnesium alloy 被引量:7
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作者 M.DAREINI A.H.JABBARI m.sedighi 《Transactions of Nonferrous Metals Society of China》 SCIE EI CAS CSCD 2020年第5期1249-1266,共18页
The effect of hot-forging process was investigated on microstructural and mechanical properties of AZ31 B alloy and AZ31 B/1.5 vol.%Al2 O3 nanocomposite under static and cycling loading. The as-cast alloy and composit... The effect of hot-forging process was investigated on microstructural and mechanical properties of AZ31 B alloy and AZ31 B/1.5 vol.%Al2 O3 nanocomposite under static and cycling loading. The as-cast alloy and composite were firstly subjected to a homogenization heat treatment at 450 ℃ and then an open-die forging at 450 ℃. The results indicated that the presence of reinforcing particles led to grain refinement and improvement of dynamic recrystallization. The forging process was more effective to eliminate the porosity in the cast alloy workpiece. Microhardness of the forged composite was increased by up to 80% and 16%, in comparison with those of the cast and forged alloy samples, respectively. Ultimate tensile strength and maximum tensile strain of the composite were improved by up to 45% and 23%, compared with those of the forged alloy in similar regions. These enhancements were respectively 50% and 37% in the compression test. The composite exhibited a fatigue life improvement in the region with low applied strain;however, a degradation was observed in the high applied strain region. Unlike AZ31 B samples, tensile, compressive and high cycle fatigue behaviors of the composite showed less sensitivity to the applied strain, which can be attributed to the amount of porosity in the samples before and after the hot-forging. 展开更多
关键词 magnesium matrix nanocomposite AZ31B alloy nano-sized Al2O3 open-die hot-forging high cycle fatigue mechanical properties microstructural evolution
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In vitro corrosion-fatigue behavior of biodegradable Mg/HA composite in simulated body fluid 被引量:2
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作者 E.Ghazizadeh A.H.Jabbari m.sedighi 《Journal of Magnesium and Alloys》 SCIE EI CAS CSCD 2021年第6期2169-2184,共16页
Magnesium and its composites as biodegradable materials offer especial capabilities to be used as bio-absorbable implants.However,their poor corrosion and fatigue properties in the physiological environment can restri... Magnesium and its composites as biodegradable materials offer especial capabilities to be used as bio-absorbable implants.However,their poor corrosion and fatigue properties in the physiological environment can restrict their applications.In this study,corrosion-fatigue tests have been performed on the extruded magnesium and magnesium/hydroxyapatite(Mg/HA)composites in a high cycle regime.To produce the composites,pure magnesium was reinforced by 2.5 wt.%and 5 wt.%of hydroxyapatite submicron particles using an electromagneticmechanical stirring method and hot extrusion process.The experimental density measurement exhibits that the porosity increases in the extruded samples with more hydroxyapatite particles.To investigate the corrosion and corrosion-fatigue behavior of the specimens,simulated body fluid(SBF)was used during in vitro tests.The results of the potentiodynamic polarization corrosion test show that the composite with 2.5 wt.%of hydroxyapatite(Mg/2.5 wt.%HA)and the pure magnesium specimen exhibit the highest and the lowest corrosion resistance,respectively.Regarding the elemental mapping analysis of the corroded samples,this behavior could be due to the formation of strong phosphorus-calcium based layers on the composite surface.The results obtained from the mechanical tests indicate that Mg/5 wt.%HA offered the highest tensile and compressive yield strengths,as well as the most promising high cycle fatigue behavior.During the corrosionfatigue test,the simultaneous effects of fatigue and corrosion damages led to a similar corrosion-fatigue behavior in both composites.The fracture surfaces of the corrosion-fatigue samples suggest that the cracks are initiated in the corroded regions of the samples surface,which reduces the crack initiation step and subsequently decreases the fatigue life.In comparison with the pure magnesium,both composites exhibit more promising corrosion and corrosion-fatigue behaviors with a significant fatigue life improvement in the physiological environment. 展开更多
关键词 MAGNESIUM Magnesium/Hydroxyapatite composite CORROSION BIODEGRADATION High cycle fatigue Corrosion-fatigue
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应变路径对AA1050铝板力学性能、成形极限曲线及织构演化影响的实验研究 被引量:2
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作者 A.ROUZBEH S.M.ATIFEH +1 位作者 m.sedighi R.HASHEMI 《Journal of Central South University》 SCIE EI CAS CSCD 2023年第8期2472-2484,共13页
实验研究了应变路径变化对AA1050铝合金力学性能、成形性能和成形极限的影响。讨论了以单向、反向和交叉轧制的三种不同方式的应变路径。对比了三种轧制方式在20%和40%轧制比下的晶粒尺寸、硬度、应力-应变曲线和成形极限。结果表明,交... 实验研究了应变路径变化对AA1050铝合金力学性能、成形性能和成形极限的影响。讨论了以单向、反向和交叉轧制的三种不同方式的应变路径。对比了三种轧制方式在20%和40%轧制比下的晶粒尺寸、硬度、应力-应变曲线和成形极限。结果表明,交叉轧制试样的晶粒尺寸小于其他方式轧制试样的晶粒尺寸;单向和交叉轧制试样的强度和伸长率均高于反向轧制方式的,单向和交叉轧制试样的硬度等于或大于反向轧制试样的;此外,交叉轧制使试样的各向异性减小,R趋近于1。试样的成形极限在交叉轧制方式下明显提高,在40%轧制比下,交叉轧制的FLC_(0)为0.113,单向轧制的FLC_(0)为0.09,反向轧制的FLC_(0)为0.081。单向和反向轧制的成形极限与加载路径的相关。 展开更多
关键词 应变路径 成形性 轧制方向 织构演变 铝合金板
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Effect of stiffeners on crashworthiness of square aluminium columns considering damage evolution 被引量:1
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作者 H.R.Allahbakhsh M.Shariati m.sedighi 《Journal of Central South University》 SCIE EI CAS 2013年第3期599-607,共9页
Combining the optimization and FEM technology,crashworthiness of aluminum extrusions was studied for an automobile safety plan.The effects of longitudinal stiffeners on the crushing of stiffened square columns were st... Combining the optimization and FEM technology,crashworthiness of aluminum extrusions was studied for an automobile safety plan.The effects of longitudinal stiffeners on the crushing of stiffened square columns were studied considering the damage evolution.The numerical analysis was carried out by ABAQUS software.Subsequently,the collapse behavior of aluminum extrusion damage was validated by comparing against solution published in literature.Finally,in order to find more efficient and lighter crush absorber and achieving minimum peak crushing force,response surface methodology(RSM) has been applied for optimizing the aluminum extrusion tube. 展开更多
关键词 damage response surface methodology (RSM) CRASHWORTHINESS STIFFENER
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Process parameter effects on microstructure and mechanical properties of tubes processed via friction assisted tube straining method
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作者 S.H.HOSSEINI m.sedighi 《Journal of Central South University》 SCIE EI CAS CSCD 2021年第10期3008-3017,共10页
This paper investigates process parameter effects on microstructure and mechanical properties of the tubes processed via recently developed friction assisted tube straining(FATS)method.For this purpose,design of exper... This paper investigates process parameter effects on microstructure and mechanical properties of the tubes processed via recently developed friction assisted tube straining(FATS)method.For this purpose,design of experiment was used to arrange finite element analyses and experimental tests.Numerical and experimental tests were executed by changing rotary speed,feed rate and die angle.Taguchi design results show that increasing feed rate and decreasing rotary speed enhance Zener-Hollomon(Z)parameter and decrease average grain size,while die angle has no considerable effect.Increasing Z value reduces grain size and enhances flow stress of the processed samples,while the experiment with the highest Z value refines initial microstructure from 40 to 8μm and increases flow stress by 5 times. 展开更多
关键词 friction assisted tube straining process parameter MICROSTRUCTURE Taguchi method finite element simulation
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