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高效液相色谱法测定盐酸赛庚啶注射液中药物含量及有关物质 被引量:2
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作者 刘婷 杨茜 +5 位作者 高立军 闫海涛 高静 张慧 王汀 郑爱萍 《国际药学研究杂志》 CAS 北大核心 2019年第11期873-878,共6页
目的建立测定盐酸赛庚啶注射液中药物含量和有关物质的高效液相色谱方法。方法药物含量测定采用COSMOSIL C8色谱柱(4.6 mm×250 mm,5μm),流动相为乙腈-磷酸盐缓冲液(0.045 mol/L,pH 4.5)(42∶58,V/V),流速为1.0 ml/min,进样量为20... 目的建立测定盐酸赛庚啶注射液中药物含量和有关物质的高效液相色谱方法。方法药物含量测定采用COSMOSIL C8色谱柱(4.6 mm×250 mm,5μm),流动相为乙腈-磷酸盐缓冲液(0.045 mol/L,pH 4.5)(42∶58,V/V),流速为1.0 ml/min,进样量为20μl,检测波长为286 nm。参考2015版《中华人民共和国药典》,有关物质测定也采用HPLC方法,除了采用梯度洗脱、检测波长设定为230 nm等不同之外,其他色谱条件同药物含量测定。用本文研究建立的上述HPLC方法,测定3批自制盐酸赛庚啶注射液样品中药物含量,并开展稳定性研究。结果建立的HPLC药物含量测定方法在盐酸赛庚啶10~40μg/ml范围内线性关系良好(Y=40.551X+13.869,r=0.9999),平均回收率为99.00%(RSD=0.39%)。在测定有关物质的HPLC条件下,盐酸赛庚啶与杂质得到良好分离,辅料不干扰测定。结论建立的HPLC方法简便、准确、灵敏度高、专属性强,可用于盐酸赛庚啶注射液中药物含量及有关物质测定。 展开更多
关键词 盐酸赛庚啶 高效液相色谱法 含量 有关物质 稳定性
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卡巴优化设置及常见问题解答
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作者 liuting 《网络与信息》 2007年第5期56-56,共1页
俄罗斯的卡巴斯基是全球最著名最强大的反病毒软件之一。但是其资源占用方面一直为人所诟病。其实卡巴斯基经过合理的设置之后。并不比其他杀毒软件占用系统资源多。下面我就说说卡巴斯基的设置问题。
关键词 优化设置 问题解答 卡巴斯基 资源占用 反病毒软件 杀毒软件 俄罗斯
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Effect of Respiratory Function Training on Pulmonary Function in Patients with Rheumatic Heart Disease
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作者 liuting XIEJiaxiang 《外文科技期刊数据库(文摘版)医药卫生》 2022年第4期127-131,共5页
Objective: to explore the effect of respiratory function training on improving pulmonary function in patients with rheumatic heart disease. Methods: 61 patients with rheumatic heart disease received by the cardiac sur... Objective: to explore the effect of respiratory function training on improving pulmonary function in patients with rheumatic heart disease. Methods: 61 patients with rheumatic heart disease received by the cardiac surgery department of the hospital from April 11, 2020 to April 11, 2021 were grouped according to the time of elective heart surgery. 30 patients in the traditional group received traditional nursing intervention and 31 patients in the experimental group received respiratory function training. The postoperative pulmonary function and postoperative adverse reactions of the two groups were observed. Results: before nursing, the forced expiratory volume (FEV1), respiratory volume (FVC), the percentage of forced vital capacity in forced vital capacity (FEV1%) in the first second and the level of blood oxygen saturation (SaO2) in the two groups were highly homogeneous. After nursing, the levels of FEV1, FVC, FEV1% and SaO2 in the two groups were higher than those before nursing. FEV1, FVC The level of FEV1% was significantly higher than that of the traditional group, the statistical predictive value showed that there was specificity (P < 0.05), the level of SaO2 was slightly higher than that of the traditional group, and the statistical predictive value showed that there was no specificity (P > 0.05);The incidence of sputum cough and aspiration pneumonia in the experimental group was lower than that in the traditional group. The statistical prediction results showed that there was specificity (P < 0.05);The comparison of the satisfaction questionnaire between the two groups shows that the average score of the satisfaction questionnaire in the experimental group is higher than that in the traditional group, and the statistical prediction results suggest that there is specificity (P < 0.05). Conclusion: preoperative respiratory function training for rheumatic heart disease is helpful to the recovery of postoperative pulmonary function, reduce postoperative adverse reactions and improve patients satisfaction with medical services, which can be used as an important auxiliary measure before heart surgery. 展开更多
关键词 rheumatic heart disease heart surgery respiratory function training pulmonary function
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Research on the English Teaching Strategy in Junior High School under the "Double Reduction Policy"
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作者 liuting 《外文科技期刊数据库(文摘版)教育科学》 2022年第3期133-136,共4页
The purpose of the double reduction policy is to reduce the homework burden and off-campus training burden for students in the compulsory education stage, abide by the development rules of students and education, focu... The purpose of the double reduction policy is to reduce the homework burden and off-campus training burden for students in the compulsory education stage, abide by the development rules of students and education, focus on the healthy development of students' physical and mental health, provide students with rest time, and comprehensively improve the quality of school classroom teaching. In the face of the implementation of the double reduction policy, junior middle school English teachers need to actively innovate the teaching concept and teaching mode, and do a good job of effective teaching strategy research, in order to help strengthen the efficiency of junior middle school English classroom teaching efficiency. This paper mainly analyzes the English teaching strategy of junior middle schools under the double reduction policy, in order to deepen the reform of English teaching and improve the effectiveness of classroom teaching. 展开更多
关键词 double reduction policy junior high school English teaching strategy
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