Stoichiometric hydroxyapatite(HA)nanoparticles were synthesized by a wet chemical method.Calcium nitrate tetra hydrate used as calcium source and dibasic ammonium phosphate used as phosphorous source.Calcium nitrate t...Stoichiometric hydroxyapatite(HA)nanoparticles were synthesized by a wet chemical method.Calcium nitrate tetra hydrate used as calcium source and dibasic ammonium phosphate used as phosphorous source.Calcium nitrate tetra hydrate and dibasic ammonium phosphate solutions were prepared by dissolving the salts in distilled water.Stoichiometric hydroxyapatite nanoparticles used by artificial bone powders and synthesized by a wet chemical method were analyzed using EDXRF method.The concentrations of K,Ca,Ti,V,Cr,Fe,Ni,Cu,Sr and Pb for artificial bone powders have been determined.Besides,Calcium contents were evaluated according to the agitation time and temperature in the production process.展开更多
The electronic structures of Ni-Ti shape-memory alloy samples were investigated by X-ray absorption fine structure （XAFS） spectroscopy both experimentally and theoretically. In the experimental section, the samples ...The electronic structures of Ni-Ti shape-memory alloy samples were investigated by X-ray absorption fine structure （XAFS） spectroscopy both experimentally and theoretically. In the experimental section, the samples were measured at low temperature to determine the persistent traces of both preheating process and atomic concentration effects on the crystal and electronic structure by X-ray absorption near-edge structure （XANES） spectroscopy. As a second step, the extended-X-ray absorption fine structure （EXAFS） calculations, which are based on different choices of one electron potentials according to Ti coordinations by using the real space multiple scattering method FEFF 8.2 code, were performed. The crystallographic and electronic structures of the porous Ni-Ti alloys were tested at various temperatures ranging from 5 to 1323 K.展开更多
文摘Stoichiometric hydroxyapatite(HA)nanoparticles were synthesized by a wet chemical method.Calcium nitrate tetra hydrate used as calcium source and dibasic ammonium phosphate used as phosphorous source.Calcium nitrate tetra hydrate and dibasic ammonium phosphate solutions were prepared by dissolving the salts in distilled water.Stoichiometric hydroxyapatite nanoparticles used by artificial bone powders and synthesized by a wet chemical method were analyzed using EDXRF method.The concentrations of K,Ca,Ti,V,Cr,Fe,Ni,Cu,Sr and Pb for artificial bone powders have been determined.Besides,Calcium contents were evaluated according to the agitation time and temperature in the production process.
基金partly supported by BIDEB-2219 grant of TUBITAK,Turkey and ADYUBAP,Turkey
文摘The electronic structures of Ni-Ti shape-memory alloy samples were investigated by X-ray absorption fine structure （XAFS） spectroscopy both experimentally and theoretically. In the experimental section, the samples were measured at low temperature to determine the persistent traces of both preheating process and atomic concentration effects on the crystal and electronic structure by X-ray absorption near-edge structure （XANES） spectroscopy. As a second step, the extended-X-ray absorption fine structure （EXAFS） calculations, which are based on different choices of one electron potentials according to Ti coordinations by using the real space multiple scattering method FEFF 8.2 code, were performed. The crystallographic and electronic structures of the porous Ni-Ti alloys were tested at various temperatures ranging from 5 to 1323 K.
