Aluminium based composites containing 1, 1.5 and 2wt. % of nano-sized Titanium Carbide particulates (TiC), with an average of 45nm, reinforcement were synthesized using low energy planetary ball mill followed by hot e...Aluminium based composites containing 1, 1.5 and 2wt. % of nano-sized Titanium Carbide particulates (TiC), with an average of 45nm, reinforcement were synthesized using low energy planetary ball mill followed by hot extrusion. Microstructural characterization of the materials revealed uniform distribution of reinforcement, grain refinement and the presence of minimal porosity. Properties characterization revealed that the presence of nano-TiC particulates led to an increase in hardness, elastic modulus, 0.2% yield strength (0.2% offset on a stress-strain curve), and the stress at which a material exhibits a specified permanent deformation, Ultimate Tensile Strength (UTS) and ductility of pure aluminum. Fractography studies revealed that the fracture of pure aluminum occurred in ductile mode due to the incorporation and uniform distribution of nano-TiC particulates. An attempt is made in the present study to correlate the effect of nano-sized TiC particulates as reinforcement and processing type with the micro structural and tensile properties of aluminum composites. The mechanical properties, namely, the UTS, hardness, grain size and distribution of the reinforcement in the base metal were studied in as sintered and extruded conditions. Orowan strengthening criteria was used to predict the yield strength of Al-TiC composites in the present work and experimental results were compared with the theoretical results.展开更多
The present article reports on characterization studies performed on amorphized nanostructured Al 6063 alloy powder synthesized by mechanical alloying (MA). The as-milled powder was characterized by X-ray diffraction ...The present article reports on characterization studies performed on amorphized nanostructured Al 6063 alloy powder synthesized by mechanical alloying (MA). The as-milled powder was characterized by X-ray diffraction (XRD) for investigating the development of crystallite nature and determining the different phases of the materials present, scanning electron microscope (SEM) was used for in depth morphological study and High Resolution-transmission electron microscope (HR-TEM) was employed to ensure the development of a nano-structured nature of the Al 6063 matrix. In the present work alloyed powder was milled for 20 h and 40 h at 300 rpm;and 20 h at 700 rpm in a hardened stainless steel medium. Using Williamson-Hall equation;crystallite size, lattice strain and lattice parameter of Al 6063 nanostructure alloy powder was estimated with broadening of XRD peaks. XRD results showed that the crystallite size of Al 6063 alloy powder reached 32 and 53 nm after 20 h at 700 rpm and 40 h at 300 rpm respectively.展开更多
文摘Aluminium based composites containing 1, 1.5 and 2wt. % of nano-sized Titanium Carbide particulates (TiC), with an average of 45nm, reinforcement were synthesized using low energy planetary ball mill followed by hot extrusion. Microstructural characterization of the materials revealed uniform distribution of reinforcement, grain refinement and the presence of minimal porosity. Properties characterization revealed that the presence of nano-TiC particulates led to an increase in hardness, elastic modulus, 0.2% yield strength (0.2% offset on a stress-strain curve), and the stress at which a material exhibits a specified permanent deformation, Ultimate Tensile Strength (UTS) and ductility of pure aluminum. Fractography studies revealed that the fracture of pure aluminum occurred in ductile mode due to the incorporation and uniform distribution of nano-TiC particulates. An attempt is made in the present study to correlate the effect of nano-sized TiC particulates as reinforcement and processing type with the micro structural and tensile properties of aluminum composites. The mechanical properties, namely, the UTS, hardness, grain size and distribution of the reinforcement in the base metal were studied in as sintered and extruded conditions. Orowan strengthening criteria was used to predict the yield strength of Al-TiC composites in the present work and experimental results were compared with the theoretical results.
文摘The present article reports on characterization studies performed on amorphized nanostructured Al 6063 alloy powder synthesized by mechanical alloying (MA). The as-milled powder was characterized by X-ray diffraction (XRD) for investigating the development of crystallite nature and determining the different phases of the materials present, scanning electron microscope (SEM) was used for in depth morphological study and High Resolution-transmission electron microscope (HR-TEM) was employed to ensure the development of a nano-structured nature of the Al 6063 matrix. In the present work alloyed powder was milled for 20 h and 40 h at 300 rpm;and 20 h at 700 rpm in a hardened stainless steel medium. Using Williamson-Hall equation;crystallite size, lattice strain and lattice parameter of Al 6063 nanostructure alloy powder was estimated with broadening of XRD peaks. XRD results showed that the crystallite size of Al 6063 alloy powder reached 32 and 53 nm after 20 h at 700 rpm and 40 h at 300 rpm respectively.
