摘要
对电化学合成碘仿装置进行了改进，探索出了利用该装置合成碘仿的最佳反应条件。结果表明，新装置能够满足半微量有机化学实验的要求，碘仿的产率可达到54．9％。该装置具有实用性和推广价值。
In this paper, a new device of synthesizing iodoform by electrochemistry method was introduced and the optimum reaction condition of synthesizing iodoform had been explored by this device. The results showed that the device could satisfy the requirments of the semi- microorganic chemistry experiment and the yield of iodoform reach 54. 9%. The device possesses practicability and value of popularization.
出处
《实验技术与管理》
CAS
2007年第3期49-51,共3页
Experimental Technology and Management
关键词
装置
碘仿
电化学
合成
device
iodoform
electrochemistry
synthesis
