摘要
本文描述使用温梯法(TGT)生长(1102)方向的白宝石单晶,应用X射线双晶摇摆曲线(XRC)测定了晶体内部的完整性,再利用KOH熔体腐蚀出样品的r面(1102)上的位错蚀坑,借助扫描电子显微镜(SEM)进行观察,发现r面白宝石的位错腐蚀坑呈等腰三角形,并且有台阶状结构,并分析了位错的成因。
A high quality sapphire single crystal oriented along (1-↑102) was grown by the temperature gradient technique (TGT) and the crystal quality was investigated using X-ray rocking curve (XRC). The etch pits of dislocations were revealed on the r-plane (1-↑102 ) sapphire by using a melted KOH as etchants. Scanning electron microscope (SEM) demonstrates that the shapes of etch pits located in r- plane of sapphire look like a isosceles triangle with sidestep-like structure. And the mechanism of the formation of dislocations was discussed.
出处
《人工晶体学报》
EI
CAS
CSCD
北大核心
2005年第4期653-656,共4页
Journal of Synthetic Crystals
关键词
温梯法
r面白宝石
位错
化学腐蚀
腐蚀坑
缺陷
temperature gradient technique (TGT)
r-plane sapphire
dislocation
chemical etching
etch pit
defect