期刊文献+

r面白宝石单晶的温梯法生长及缺陷研究 被引量:4

Defect Study of r-plane Sapphire Single Crystal Grown by Temperature Gradient Technique
在线阅读 下载PDF
导出
摘要 本文描述使用温梯法(TGT)生长(1102)方向的白宝石单晶,应用X射线双晶摇摆曲线(XRC)测定了晶体内部的完整性,再利用KOH熔体腐蚀出样品的r面(1102)上的位错蚀坑,借助扫描电子显微镜(SEM)进行观察,发现r面白宝石的位错腐蚀坑呈等腰三角形,并且有台阶状结构,并分析了位错的成因。 A high quality sapphire single crystal oriented along (1-↑102) was grown by the temperature gradient technique (TGT) and the crystal quality was investigated using X-ray rocking curve (XRC). The etch pits of dislocations were revealed on the r-plane (1-↑102 ) sapphire by using a melted KOH as etchants. Scanning electron microscope (SEM) demonstrates that the shapes of etch pits located in r- plane of sapphire look like a isosceles triangle with sidestep-like structure. And the mechanism of the formation of dislocations was discussed.
出处 《人工晶体学报》 EI CAS CSCD 北大核心 2005年第4期653-656,共4页 Journal of Synthetic Crystals
关键词 温梯法 r面白宝石 位错 化学腐蚀 腐蚀坑 缺陷 temperature gradient technique (TGT) r-plane sapphire dislocation chemical etching etch pit defect
  • 相关文献

参考文献9

  • 1Liu L,Edgar J H. Substrates for Gallium Nitride Epitaxy [J].Materials Science and Engineering,2002,37(3):3061-127.
  • 2Ambacher O.Growth and Applications of Group Ⅲ-nitrides [J].J. Phys. D: Appl. Phys.,1998,31:2653-2710.
  • 3Xu Jianwei, Zhou Yongzong, Zhou Guoqing, Xu Ke, Deng Peizhen, Xu Jun. Growth of Large-sized Sapphire Boules by Temperature Gradient Technique (TGT)[J].Journal of Crystal Growth,1998,193:123-126.
  • 4周国清,徐科,邓佩珍,徐军,周永宗,干福熹,朱人元.温梯法生长φ110mm×80mm蓝宝石晶体位错的化学腐蚀形貌分析[J].硅酸盐学报,1999,27(6):727-733. 被引量:14
  • 5Watanabe K,Sumiyoshi Y. Relationship between Habit and Etch Figures of Corundum Crystals Grown from Molten Cryolite Flux [J].Journal of Crystal Growth,1976,32:316-326.
  • 6Robert Scheuplein,Peter Gibbs. Surface Structure in Corundum:ⅠEtching of Dislocations[J].J. Am. Ceram. Soc.,1960,43(9):458-472.
  • 7Robert Scheuplein,Peter Gibbs. Surface Structure in Corundum:ⅡDislocation Structure and Fracture of Deformed Single Crystals[J].J. Am. Ceram. Soc., 1962,45(9):439-452.
  • 8Stephens D L,Alford W J. Dislocation Structures in Single-crystal Al2O3 [J].J. Am. Ceram. Soc.,1964,47(2):81-86.
  • 9曾贵平,殷绍唐,秦青海,葛玉香.钛宝石晶体中的位错以及退火对位错的影响[J].硅酸盐学报,2001,29(2):168-171. 被引量:5

二级参考文献14

  • 1南京大学地质学系岩矿教研室.结晶学与矿物学[M].北京:地质出版社,1978.333.
  • 2[1]Aggarwal R L, et al. Residual infrared absorption in as-grown and annealed crystals of Ti: Al2O3 [ J ]. IEEE J Quant Elect,1988, 24(6): 1 003.
  • 3[2]Kokta M R. Effects and growth conditions and post-growth thermal treatment on the quality of titanium-doped sapphire[ A]. In: Budgor A B, Esterowitz L, Deshazer L G ed. Tunable SolidState Lasers Ⅱ [C]. Berlin: Spring-Verlag, 1986. 89.
  • 4[3]Keshra Sangwal. Etching of Crystal[M]. Amelinckx S, Nihoul J, ed. Netherland: North-Holland Physics Publishing, 1987.434.
  • 5[4]Cadoz J, et al. Work hardening and recovery in sapphire ( α -Al2O3) undergoing prism plane deformation [ J ]. Acta Metall,1982, 30:2 205.
  • 6[5]Peter K, et al. Slip and twinning in sapphire (α-Al2O3)[J]. J Am Cerm Soc, 1994, 77(2): 385.
  • 7[6]Heuer A H, Lagerlof K P D, et al. Slip and twinning dislocation in sapphire (α-Al2O3)[J]. Phil Mag A, 1998, 78(3): 747.
  • 8[7]Stephens D L, Alford W J. Dislocation structures in single-crystal Al2O3[J]. J Am Ceram Soc, 1964, 47: 81.
  • 9[8]Watanabe K, Sumiyoshi Y. Relationship between habit and figures of conmdum crystals grown from molten cryolite flux[J]. J Cryst Growth, 1976, 32: 316.
  • 10[9]Iwasaki K, et al. Round-Robin test of EPD measurement on undoped GaAs wafers[J]. J Cryst Growth, 1990, 103: 257.

共引文献15

同被引文献34

引证文献4

二级引证文献11

相关作者

内容加载中请稍等...

相关机构

内容加载中请稍等...

相关主题

内容加载中请稍等...

浏览历史

内容加载中请稍等...
;
使用帮助 返回顶部